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Please use this identifier to cite or link to this item: http://hdl.handle.net/2289/8086
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dc.contributor.authorNaik, Yashwanth Venkatraman-
dc.contributor.authorKariduraganavar, Mahadevappa Yallappa-
dc.contributor.authorSrinivasa, Hosapalya Thimmayya-
dc.contributor.authorSiddagangaiah, Palakshamurthy Bandrehalli-
dc.date.accessioned2023-04-26T09:17:45Z-
dc.date.available2023-04-26T09:17:45Z-
dc.date.issued2022-04-
dc.identifier.citationInorganic Chemistry Communications, 2022, Vol. 138, p109275en_US
dc.identifier.issn1387-7003-
dc.identifier.urihttp://hdl.handle.net/2289/8086-
dc.descriptionRestricted Access.en_US
dc.description.abstractIn this work, A series of facile citric acid-assisted gel combustion synthesized cubic structured nickel oxide nanoparticles (NiO NPs) filled polyaniline (PANI) were prepared via in-situ chemical oxidative polymerization method. The effect of different mass percent loaded NiO NPs on the PANI matrix and its crystalline structure, thermal stability, morphology, direct current (DC) conductivity, and electrolyte solvent affinity were investigated with the help of XRD, FTIR, TGA-DTA, SEM with EDS, UV–Vis absorption, current-voltage (I-V) characteristics, and contact angle (CA) measurements. Among all prepared nanocomposites 20 wt% loaded NiO NPs per anilinium chloride (C6H8ClN) weight (NiP3) showed the highest conductivity of about 6.09 × 10−2 S cm−1, good thermal stability over the range of 40–800 °C, and better electrolyte swelling ability with CA of 43.9°. So, this optimized nanocomposite was subjected to electrochemical analysis in 1 M HCl solution using cyclic voltammetry (CV), Galvanometric charge-discharge (GCD), electrochemical impedance spectroscopy (EIS). From 10 mV s−1 scan rated CV the Csp, Ea,c, and E(HE/OE)-pa for NiP3 voltammogram was found to be 480 F g−1, 0.4116 V, 0.7531 V respectively. Further, the results have confirmed that the specific capacitance of NiP3 was enhanced enormously than the pristine PANI.en_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.urihttps://doi.org/10.1016/j.inoche.2022.109275en_US
dc.rights2022 Elsevieren_US
dc.subjectNiOen_US
dc.subjectNPsen_US
dc.subjectPANIen_US
dc.subjectCitric acid assisted solution combustion methoden_US
dc.subjectIn-situ chemical oxidative polymerizationen_US
dc.subjectXRDen_US
dc.subjectSEMen_US
dc.subjectFTIRen_US
dc.subjectTGAen_US
dc.subjectCAen_US
dc.subjectCVen_US
dc.subjectGCDen_US
dc.subjectEISen_US
dc.titleHigh surface wetting and conducting NiO/PANI nanocomposites as efficient electrode materials for supercapacitorsen_US
dc.typeArticleen_US
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